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日用化学工业 ›› 2016, Vol. 46 ›› Issue (12): 714-717.doi: 10.13218/j.cnki.csdc.2016.12.008

• 开发与应用 • 上一篇    下一篇

化橘红黄酮提取及膏状抗氧化面膜的制备

彭颖1,2,邱松山1,莫梓杰1,周如金1   

  1. 1.广东石油化工学院 化工学院,广东 茂名 525000;
    2.华中农业大学 食品科技学院,湖北 武汉 430070
  • 出版日期:2016-12-22 发布日期:2019-04-18
  • 通讯作者: 周如金,教授,博士,电话:18929783366,E-mail:rujinzhou@126.com。
  • 作者简介:彭颖(1983-),女,湖北黄冈人,博士研究生,电话:15071209936,E-mail:pengkangying@sina.com。
  • 基金资助:
    化州科技计划资助项目(2015003);广东省科技计划资助项目(2014B040404027)

Preparation of Exocarpium Citri grandis extract and antioxidation mask

PENG Ying1,2,QIU Song-shan1,MO Zi-jie1,ZHOU Ru-jin1   

  1. 1.Chemical Engineering College,Guangdong University of Petrochemical Technology,Maoming,Guangdong 525000,China;
    2.Food Science &Technology College,Huazhong Agricultural University,Wuhan,Hubei 430070,China
  • Online:2016-12-22 Published:2019-04-18

摘要: 采用乙醇浸提法将化橘红中的黄酮提取分离得到乙醇提取物。研究了提取温度、料液比、乙醇体积分数对黄酮提取率的影响。以单因素试验为基础,通过正交试验优化了化橘红中黄酮的乙醇浸提工艺。确定较佳工艺条件为:提取温度80 ℃,料液比1∶50 (g∶mL),乙醇体积分数80%。在此条件下,黄酮的提取率为3.19%。以具有抗氧化功能的VC和没食子酸丙酯(PG)作为标准参照,将化橘红提取液加到面膜中,研制出具有抗氧化活性的面膜产品,为化橘红资源应用指出新方向。

关键词: 化妆品, 化橘红, 黄酮, 抗氧化, 面膜

Abstract: Ethanol extract containing flavonoids from Exocarpium Citri grandis was prepared by extraction using ethanol as the extraction solvent.The impact of extraction temperature,ratio of solid to liquid materials and volume fraction of the ethanol solvent on the extraction rate of flavonoids were examined.Based on the single factor tests results,the ethanol extraction process of flavonoids in Exocarpium Citri grandis was optimized by orthogonal experiment.The optimum conditions were identified as follows:extraction temperature,80 ℃;ratio of solid material to solvent (g∶mL),1∶50;and ethanol volume fraction,80%.Under these conditions,the extraction rate of flavonoids achieves 3.19%.The extract was added into the mask raw material to cause the antioxidation activity of the mask products with vitamin C and propyl gallate (PG) as standard reference,so as to develop new direction for the application of local orange resources.

Key words: cosmetics, Exocarpium Citri grandis, flavonoids, antioxidant, mask

中图分类号: 

  • TQ658