超声制备甲醇柴油乳液及其稳定性研究

doi:10.13218/j.cnki.csdc.2015.10.007

日用化学工业 ›› 2015, Vol. 45 ›› Issue (10): 568-571.doi: 10.13218/j.cnki.csdc.2015.10.007

超声制备甲醇柴油乳液及其稳定性研究

焦纬洲, 李晓霞, 李鹏, 何守琪, 符曼, 王永明

中北大学山西省超重力化工工程技术研究中心,山西太原 030051

收稿日期:2015-05-08 修回日期:2015-09-24 出版日期:2015-10-22 发布日期:2019-04-10
作者简介:焦纬洲(1981-),男,山西人,博士,教授,电话:(0351)3921986,E-mail:jwz0306@126.com。
基金资助:
国家自然科学基金资助项目(21206153)

Preparation and stability of methanol diesel oil emulsion under action of ultrasonic wave

JIAO Wei-zhou, LI Xiao-xia, LI Peng, HE Shou-qi, FU Man, WANG Yong-ming

Research Center of Shanxi Province for High Gravity Chemical Engineering and Technology,North University of China,Taiyuan,Shanxi 030051,China

Received:2015-05-08 Revised:2015-09-24 Online:2015-10-22 Published:2019-04-10

摘要/Abstract

摘要： 采用Tween 80,Span 80,Tween 20,油酸和十二烷基磺酸钠复配作为乳化剂,利用高速分散器和超声波装置作为预乳化和深度乳化装置制备甲醇柴油乳液。研究了超声参数(声强和作用时间)、乳化剂及甲醇用量等对甲醇柴油乳液稳定性的影响,得出适宜的操作条件为:复配乳化剂HLB值为5.1,复配乳化剂质量分数为3%,甲醇体积分数为15%,预乳化时间为5 min,转速为5×2 800 r/min,超声乳化时间为15 min,超声作用功率为352 W。

关键词: 乳化剂, 甲醇柴油乳液, 超声波, 稳定性

Abstract: Adopting blends of Tween 80,Span 80,Tween 20,oleic acid and sodium dodecyl sulfate as emulsifier,methanol diesel oil emulsion was prepared with high speed dispersing machine and ultrasonic wave device.Effect of the ultrasonic parameters (ultrasonic wave intensity,duration of ultrasonic wave treatment),dosage of emulsifier and methanol on the stability of methanol diesel oil emulsion was investigated.The suitable operating conditions were determined as following:HLB value,5.1;emulsifying agent mass fraction,3%;methanol volume fraction,15%;high speed dispersing time,5 min;speed of the dispersing machine,5×2 800 r/min;duration of ultrasonic wave treatment,15 min;power of the ultrasonic wave device,352 W.

Key words: emulsifier, methanol diesel oil emulsion, ultrasonic, stability

中图分类号:

TQ423.92

焦纬洲, 李晓霞, 李鹏, 何守琪, 符曼, 王永明. 超声制备甲醇柴油乳液及其稳定性研究[J]. 日用化学工业, 2015, 45(10): 568-571.

JIAO Wei-zhou, LI Xiao-xia, LI Peng, HE Shou-qi, FU Man, WANG Yong-ming. Preparation and stability of methanol diesel oil emulsion under action of ultrasonic wave[J]. China Surfactant Detergent & Cosmetics, 2015, 45(10): 568-571.

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超声制备甲醇柴油乳液及其稳定性研究

Preparation and stability of methanol diesel oil emulsion under action of ultrasonic wave

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