抗菌纤维的抑菌活性及其在面膜产品中的应用研究

doi:10.3969/j.issn.2097-2806.2023.05.007

摘要/Abstract

摘要：

对抗菌纤维和多种抑菌成分的复配样品进行抑菌性能测试，并对比了季铵盐壳聚糖抗菌纤维与植物精油、传统防腐剂和防腐替代剂对细菌、酵母菌和霉菌的抑制效果，尝试将抗菌纤维和抑菌成分形成复配防腐方案。防腐测试结果表明：抗菌纤维与对羟基苯乙酮（0.1%-质量分数，下同），或丁香油（0.05%），或柠檬茶树油，以及蓝桉叶油复配，均能满足面膜产品的防腐需求。但是，抗菌纤维与羟苯甲酯复配有拮抗作用。其中，抗菌纤维与丁香油（0.05%）复配，抑菌效果最佳。抑菌纤维还能显著提升植物精油的抑菌效果，对丁香油的提升率达43.06%。

关键词: 抗菌纤维, 抑菌性能, 面膜防腐, 植物精油, 对羟基苯乙酮

Abstract:

To reduce irritant and toxicity risk effectively caused by traditional cosmetics preservatives, chitosan quaternary ammonium salt-based antibacterial fiber combined with several various bacteriostatic ingredients was constructed to replace the traditional preservatives used in facial mask products, which obviously improved its broad-spectrum antibacterial ability. The antibacterial properties of antibacterial fiber combined with a variety of antibacterial components were tested. The antibacterial effects comparison among quaternary ammonium chitosan antibacterial fiber combined with plant essential oil, traditional preservatives, and antiseptic substitutes on bacteria, yeast and mold was conducted. The several antiseptic recipes include antibacterial fiber and different antibacterial components were proposed. Antibacterial test results show that the antibacterial fiber combined with hydroxyacetophenone （0.1%-mass fraction, the same below）, or Eugenia caryophyllus Thunb. oil （0.05%）, or Leptospermum petersonii FM. Bailey oil, or Eucalyptus globulus Labill. oil, can meet the antibacterial requirements of mask products. However, the antibacterial fiber combined with methylparaben has antagonistic effect. Among them, the combination of antibacterial fiber with Eugenia caryophyllus Thunb. oil（0.05%） has the best antibacterial effect. The antibacterial fiber can significantly improve the antibacterial effect, and the improvement rate of Eugenia caryophyllus Thunb. oil is 43.06%.

Key words: antibacterial fiber, bacteriostatic performance, mask anticorrosion, essential oil, hydroxyacetophenone

中图分类号:

TQ658

孔秋婵, 蒋佳欣, 夏高辉, 龚盛昭. 抗菌纤维的抑菌活性及其在面膜产品中的应用研究[J]. 日用化学工业（中英文）, 2023, 53(5): 538-543.

Kong Qiuchan, Jiang Jiaxin, Xia Gaohui, Gong Shengzhao. Study on antibacterial activity of antibacterial fiber and its application in mask products[J]. China Surfactant Detergent & Cosmetics, 2023, 53(5): 538-543.

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抑菌圈宽度/mm	抑菌物质溶出性
≤1	非溶出性
>1~≤5	微溶出性
>5~≤10	中等溶出性
>10	高溶出性

细菌和酵母菌			真菌
菌种	抑菌率	抗菌效果	抑菌值A/培养后真菌数Tt	抗真菌效果
金黄色葡萄球菌	≥70%	有效	A<1	无效
大肠杆菌	≥70%	有效	1≤A<2	轻微抗菌
白色假丝酵母	≥60%	有效	2≤A<3	中等抗菌
铜绿假单胞菌	≥70%	有效	A≥3	全效抗菌
			Tt=0	杀真菌

类型	成分	编码	w/%
植物精油	丁香油	#1	0.03
	丁香油	#8	0.05
	茶树油	#2	0.03
	柠檬茶树油	#3	0.03
	柠檬茶树油	#9	0.05
	迷迭香叶油	#4	0.03
	蓝桉叶油	#5	0.03
	蓝桉叶油	#10	0.05
传统防腐剂	羟苯甲酯	#6	0.10
防腐替代剂	对羟基苯乙酮	#7	0.10
阳性对照	羟苯甲酯	#11	0.12
阳性对照	羟苯丙酯	#11	0.02

菌种	抑菌圈宽度/mm	抑菌物质溶出性
金黄色葡萄球菌	0	非溶出性
大肠杆菌	0	非溶出性
白色假丝酵母	0	非溶出性

细菌和酵母菌			真菌
菌种	抑菌率/%	抗菌效果	抑菌值A	抗真菌效果
金黄色葡萄球菌	92.14	有效	A=0.195	无效
大肠杆菌	93.75	有效
白色假丝酵母	63.64	有效
铜绿假单胞菌	90.00	有效