HPLC法同时测定化妆品中补骨脂素、异补骨脂素、新补骨脂异黄酮和补骨脂二氢黄酮含量

doi:10.3969/j.issn.1001-1803.2019.12.012

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China Surfactant Detergent & Cosmetics ›› 2019, Vol. 49 ›› Issue (12): 835-838.doi: 10.3969/j.issn.1001-1803.2019.12.012

• Analytical methods and testing • Previous Articles

HPLC determination of psoralen, lsopsoralen, neobavaisoflavone and bavachin in cosmetics

FAN Fei,LI Jing-jing,LU Bang-mei

XI’an Institute for Food and Drugs Control, Xi’an, Shaanxi 710054, China

Received:2019-04-03 Revised:2019-11-21 Online:2019-12-22 Published:2019-12-24

Abstract

Abstract:

An analytical method for the simultaneous determination of psoralen, lsopsoralen, neobavaisoflavone and bavachin in cosmetics by HPLC were developed. The linear relationships are good in the ranges of 0.109 1-21.814 4 mg/L, 0.106 7-21.332 8 mg/L, 0.108 6-21.712 8 mg/L and 0.112 3-22.464 4 mg/L for the four components, respectively. The average recoveries are 94.78%-104.74% with the RSD less than 5%.

Key words: cosmetic, HPLC, psoralen, lsopsoralen, neobavaisoflavone, bavachin

CLC Number:

TQ658

FAN Fei,LI Jing-jing,LU Bang-mei. HPLC determination of psoralen, lsopsoralen, neobavaisoflavone and bavachin in cosmetics[J].China Surfactant Detergent & Cosmetics, 2019, 49(12): 835-838.

组分	紧肤水		乳液		蜜粉
组分	回收率/%	RSD/%	回收率/%	RSD/%	回收率/%	RSD/%
补骨脂素	98.45	0.04	99.39	0.86	100.56	0.92
	98.38	0.18	95.84	3.61	97.98	1.47
	98.43	0.61	98.00	4.57	102.57	0.23
异补骨脂素	98.21	0.01	99.40	0.66	100.71	0.82
	102.50	0.85	94.78	1.66	99.60	0.85
	99.59	0.25	99.08	2.65	101.28	0.24
新补骨脂异黄酮	98.12	0.06	100.09	0.63	102.21	0.39
	104.74	0.40	97.28	4.18	102.00	4.69
	98.27	0.41	97.76	2.89	103.18	0.28
补骨脂二氢黄酮	98.13	0.14	97.75	0.75	102.53	0.60
	101.65	0.74	97.91	1.02	103.27	0.48
	99.01	0.61	97.89	1.72	101.14	0.28

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HPLC determination of psoralen, lsopsoralen, neobavaisoflavone and bavachin in cosmetics

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