China Surfactant Detergent & Cosmetics ›› 2019, Vol. 49 ›› Issue (1): 5-7.doi: 10.3969/j.issn.1001-1803.2019.01.002
• Lecture of science and technology • Previous Articles Next Articles
HE Wen-dan1,2,LIU Lei1,2,YANG Shu-yan1,2,TANG Ying1,2
Received:
2018-11-22
Online:
2019-01-20
Published:
2019-03-06
CLC Number:
Wen-dan HE,Lei LIU,Shu-yan YANG,Ying TANG. Efficacy evaluation of cosmetics (XI)Application of in vitro techniques in the efficacy evaluation of hair cosmetics[J].China Surfactant Detergent & Cosmetics, 2019, 49(1): 5-7.
Tab. 1
In vitro techniques commonly used for the efficacy evaluation of hair cosmetics"
试验技术/模型 | 检测指标 | 评价功效 | 参考文献 |
---|---|---|---|
扫描电子显微镜 | 毛发表面的微观形貌 | 染色、清洁、防晒、修复 | [3-5] |
透射电子显微镜 | 毛发内部微观结构 | 染色、防晒、修复 | [4, 6, 7] |
原子力显微镜 | 毛发表面和内部微观结构 毛发表面粗糙度、摩擦力、附着力 | 防晒、修复 清洁、修复、定型 | [8-10] |
光学相干断层扫描 | 毛发表面和内部微观结构 | 染色、防晒、修复 | [12, 13] |
紫外可见光谱 | 生色团变化 | 染色、固色、修复 | [5, 14-16] |
荧光光谱 | 蛋白质损失 | 防晒、修复 | [5, 14, 17] |
傅里叶变换红外光谱 | 官能团变化 | 染色、防晒、修复 | [14, 18, 48] |
拉曼光谱 | 官能团变化 | 染色、防晒、修复 | [19-23] |
质谱 | 蛋白质修饰和损失 | 防晒、修复 | [24] |
色谱 | 蛋白质损失 | 防晒、修复 | [26, 27] |
扫描差热分析法 | 角蛋白变性温度、变性晗 | 防晒、修复 | [28, 29] |
拉伸性分析 | 拉伸强度、断裂应力 | 修复、定型 | [32] |
摩擦力测试 | 摩擦系数 | 修复、梳理 | [35] |
毛发梳理性 | 梳理功 | 修复、梳理 | [37] |
细胞模型(HaCaT和DP) 黑色素细胞 | 细胞增殖、基因表达 黑色素含量 | 育发 固色 | [42, 49] |
离体毛囊培养系统 | 毛发生长速率、毛发生长期 | 育发 | [47] |
微生物模型(马拉色菌) | 抑菌能力 | 抗菌、去屑 | [44, 46, 50] |
[1] |
Antunes E, Cruz C F, Azoia N G , et al. Insights on the mechanical behavior of keratin fibrils[J]. International Journal of Biological Macromolecules, 2016,89:477-483.
doi: 10.1016/j.ijbiomac.2016.05.018 pmid: 27164495 |
[2] |
Ali N, Zohra R R, Qader S A , et al. Scanning electron microscopy analysis of hair index on Karachi’s population for social and professional appearance enhancement[J]. International Journal of Cosmetic Science, 2015,37(3) : 312-320.
doi: 10.1111/ics.12201 pmid: 25639338 |
[3] |
Thibaut S, De B E, Bernard B A , et al. Chronological ageing of human hair keratin fibres[J]. Int J Cosmet Sci, 2010,32(6) : 422-434.
doi: 10.1111/j.1468-2494.2009.00570.x pmid: 20384898 |
[4] |
Ahn H J, Lee W S . An ultrastuctural study of hair fiber damage and restoration following treatment with permanent hair dye[J]. International Journal of Dermatology, 2010,41(2) : 88-92.
doi: 10.1046/j.1365-4362.2002.01375.x pmid: 11982643 |
[5] |
Fernández E, Martínezteipel B, Armengol R , et al. Efficacy of antioxidants in human hair[J]. Journal of Photochemistry & Photobiology B: Biology, 2012,117:146-156.
doi: 10.1016/j.jphotobiol.2012.09.009 pmid: 23123594 |
[6] |
Richena M, Rezende C A . Morphological degradation of human hair cuticle due to simulated sunlight irradiation and washing[J]. Journal of Photochemistry & Photobiology B: Biology, 2016,161:430-440.
doi: 10.1016/j.jphotobiol.2016.06.002 pmid: 27318298 |
[7] |
Kim M M . Effect of procyandin oligomers on oxidative hair damage[J]. Skin Research and Technology, 2011,17(1) : 108-118.
doi: 10.1111/j.1600-0846.2010.00476.x pmid: 21226878 |
[8] |
Chen N, Bhushan B . Morphological, nanomechanical and cellular structural characterization of human hair and conditioner distribution using torsional resonance mode with an atomic force microscope[J]. Journal of Microscopy, 2010,220(2) : 96-112.
doi: 10.1111/j.1365-2818.2005.01517.x pmid: 16313489 |
[9] |
Smith J R, Tsibouklis J, Nevell T G , et al. AFM friction and adhesion mapping of the substructures of human hair cuticles[J]. Applied Surface Science, 2013,285(21) : 638-644.
doi: 10.1016/j.apsusc.2013.08.104 |
[10] |
Clifford C A, Sano N, Doyle P , et al. Nanomechanical measurements of hair as an example of micro-fibre analysis using atomic force microscopy nanoindentation[J]. Ultramicroscopy, 2012,114(4) : 38-45.
doi: 10.1016/j.ultramic.2012.01.006 pmid: 22356787 |
[11] | Velasco M V, Baby A R, Sarruf F D , et al. Prospective ultramorphological characterization of human hair by optical coherence tomography[J]. Skin Research & Technology, 2010,15(4) : 440-443. |
[12] |
Camacho-Bragado G A, Balooch G, Dixon-Parks F , et al. Understanding breakage in curly hair[J]. British Journal of Dermatology, 2015,173(2) : 10-16.
doi: 10.1111/bjd.13241 pmid: 26207659 |
[13] |
Velasco M V R, Freitas A Z, Bedin V , et al. Optical coherence tomography to evaluate the effects of oxidative hair dye on the fiber[J]. Skin Research & Technology, 2016,22(4) : 430-436.
doi: 10.1111/srt.12283 pmid: 26792514 |
[14] |
Tang Y, Smith G J . Spectroscopic investigation of human hair from Chinese subjects during UVA photoageing[J]. Spectroscopy and Spectral Analysis, 2016,36(6) : 1783-1788.
doi: 10.3964/j.issn.1000-0593(2016)06-1783-06 |
[15] |
Dario M F, Baby A R, Velasco M V . Effects of solar radiation on hair and photoprotection[J]. Journal of Photochemistry & Photobiology B: Biology, 2015,153:240-246.
doi: 10.1016/j.jphotobiol.2015.09.025 pmid: 26454659 |
[16] |
Pires-Oliveira R, Joekes I . UV-vis spectra as an alternative to the Lowry method for quantify hair damage induced by surfactants[J]. Colloids & Surfaces B: Biointerfaces, 2014,123:326-330.
doi: 10.1016/j.colsurfb.2014.09.035 pmid: 25277290 |
[17] |
Estibalitz Fernández, Clara Barba, Cristina Alonso , et al. Photodamage determination of human hair[J]. Journal of Photochemistry & Photobiology B: Biology, 2012,106(1) : 101-106.
doi: 10.1016/j.jphotobiol.2011.10.011 pmid: 22119660 |
[18] |
Miyamae Y, Yamakawa Y, Ozaki Y . Evaluation of physical properties of human hair by diffuse reflectance near-infrared spectroscopy[J]. Applied Spectroscopy, 2007,61(2) : 212.
doi: 10.1366/000370207779947503 pmid: 17331314 |
[19] |
Mv F, Nn B, Ay C , et al. Photoinduced formation of thiols in human hair[J]. Journal of Photochemistry & Photobiology B: Biology, 2016,164:43-48.
doi: 10.1016/j.jphotobiol.2016.09.021 pmid: 27643983 |
[20] |
Kuzuhara A . Analysis of structural changes in permanent waved human hair using Raman spectroscopy[J]. Biopolymers, 2010,85(3) : 274-283.
doi: 10.1002/bip.20646 pmid: 17143860 |
[21] |
Kuzuhara A . Internal structural changes in keratin fibres resulting from combined hair waving and stress relaxation treatments: a Raman spectroscopic investigation[J]. International Journal of Cosmetic Science, 2016,38(2) : 201-209.
doi: 10.1111/ics.12278 pmid: 26383008 |
[22] |
Kuzuhara A, Fujiwara N, Hori T . Analysis of internal structure changes in black human hair keratin fibers with aging using Raman spectroscopy[J]. Biopolymers, 2010,87(2/3) : 134-140.
doi: 10.1002/bip.20805 pmid: 17626296 |
[23] |
Akio Kuzuhara . Analysis of structural changes in bleached keratin fibers (black and white human hair) using Raman spectroscopy[J]. Biopolymers, 2010,81(6) : 506-514.
doi: 10.1002/bip.20453 pmid: 16425172 |
[24] |
Dario M F, Freire T B, Caso P , et al. Tryptophan and kynurenine determination in human hair by liquid chromatography[J]. Journal of Chromatography B: Analytical Technologies in the Biomedical & Life Sciences, 2017,1065:59-62.
doi: 10.1016/j.jchromb.2017.09.020 pmid: 28946126 |
[25] |
Khumalo N P, Janet S, Freedom G , et al. ‘Relaxers’ damage hair: evidence from amino acid analysis[J]. Journal of the American Academy of Dermatology, 2010,62(3) : 409-410.
doi: 10.1016/j.jaad.2009.07.020 pmid: 20159307 |
[26] |
Dyer J M, Bell F, Koehn H , et al. Redox proteomic evaluation of bleaching and alkali damage in human hair[J]. International Journal of Cosmetic Science, 2013,35(6) : 555-561.
doi: 10.1111/ics.12076 pmid: 23802755 |
[27] |
Tang Y, Dyer J M, Deb-Choudhury S , et al. Trace metal ions in hair from frequent hair dyers in China and the associated effects on photo-oxidative damage[J]. Journal of Photochemistry & Photobiology B: Biology, 2016,156:35-40.
doi: 10.1016/j.jphotobiol.2016.01.010 pmid: 26803274 |
[28] |
Lima C R R D C, Machado L D B, Velasco M V R , et al. DSC measurements applied to hair studies[J]. Journal of Thermal Analysis & Calorimetry, 2018 ( 1) : 1-9.
doi: 10.1007/s10973-018-7095-0 |
[29] | Ali Kamal A, Magda Mohamed I , Mohamed Abdel-Nabi E R. Thermal analysis of some antidiabetic pharmaceutical compounds[J]. Advanced Pharmaceutical Bulletin, 2013,3(2) : 419-424. |
[30] |
Zhou Y, Rigoletto R, Koelmel D , et al. The effect of various cosmetic pretreatments on protecting hair from thermal damage by hot flat ironing[J]. Journal of Cosmetic Science, 2011,62(2) : 265.
pmid: 21635854 |
[31] |
Popescu C, Gummer C . DSC of human hair: a tool for claim support or incorrect data analysis?[J]. International Journal of Cosmetic Science, 2016,38(5) : 433-439.
doi: 10.1111/ics.12306 pmid: 26780578 |
[32] |
Yang Y, Wen Y, Wang B , et al. Structure and mechanical behavior of human hair[J]. Materials Science & Engineering C: Materials for Biological Applications, 2017,73:152.
doi: 10.1016/j.msec.2016.12.008 pmid: 28183593 |
[33] | Davis M G, Thomas J H , Velde S V D, et al . A novel cosmetic approach to treat thinning hair[J]. British Journal of Dermatology, 2015,165(S3) : 24-30. |
[34] |
Liu Yan, Liu Yijun, Hu Jinlian , et al. Development of a smart, anti-water polyurethane polymer hair coating for style setting[J]. International Journal of Cosmetic Science, 2016,38(3) : 305-311.
doi: 10.1111/ics.12294 pmid: 26584010 |
[35] |
Chevalier N R . Hair-on-hair static friction coefficient can be determined by tying a knot[J]. Colloids & Surfaces B: Biointerfaces, 2017,159:924.
doi: 10.1016/j.colsurfb.2017.08.048 pmid: 28903188 |
[36] |
Dussaud A, Fieschi-Corso L . Influence of functionalized silicones on hair fiber-fiber interactions and on the relationship with the macroscopic behavior of hair assembly[J]. International Journal of Cosmetic Science, 2010,32(2) : 155-160.
doi: 10.1111/j.1468-2494.2010.00534_15.x pmid: 19450425 |
[37] | Da G R , Franã§A-Stefoni S A, Sã-Dias T C, et al. Protective effect of conditioner agents on hair treated with oxidative hair dye[J]. J Cosmet Dermatol, 2018: 1-6. |
[38] |
Rho S-S, Park S-J, Hwang S-L , et al. The hair growth promoting effect of Asiasari radix extract and its molecular regulation[J]. Journal of Dermatological Science, 2005,38(2) : 89-97.
doi: 10.1016/s0923-1811(02)00060-9 pmid: 15862941 |
[39] |
Begum S, Lee M R, Gu L J , et al. Comparative hair restorer efficacy of medicinal herb on nude (Foxn1nu) mice[J]. Biomed Res Int, 2014,2014(6) : 319795.
doi: 10.1155/2014/319795 pmid: 25478567 |
[40] |
Woo H, Lee S, Kim S , et al. Effect of sinapic acid on hair growth promoting in human hair follicle dermal papilla cells via Akt activation[J]. Archives of Dermatological Research, 2017,309(6) : 1-8.
doi: 10.1007/s00403-016-1702-3 pmid: 27878387 |
[41] |
Liang D, Hao H, Xia L , et al. Treatment of MSCs with Wnt1a-conditioned medium activates DP cells and promotes hair follicle regrowth[J]. Sci Rep, 2014,4:5432.
doi: 10.1038/srep05432 pmid: 4069670 |
[42] |
Sextius P, Betts R, Benkhalifa I , et al. Polygonum multiflorum Radix extract protects human foreskin melanocytes from oxidative stress in vitro and potentiates hair follicle pigmentation ex vivo[J]. Int J Cosmet Sci, 2017,39(4) : 419-425.
doi: 10.1111/ics.2017.39.issue-4 |
[43] |
Soares R C, Camargo-Penna P H, Moraes V C S D , et al. Dysbiotic bacterial and fungal communities not restricted to clinically affected skin sites in dandruff[J]. Frontiers in Cellular & Infection Microbiology, 2016,6:157.
doi: 10.3389/fcimb.2016.00157 pmid: 27909689 |
[44] |
Turner G A, Matheson J R, G-Z L , et al. Enhanced efficacy and sensory properties of an anti-dandruff shampoo containing zinc pyrithione and climbazole[J]. International Journal of Cosmetic Science, 2013,35(1) : 78-83.
doi: 10.1111/ics.12007 pmid: 22970742 |
[45] | Sathishkumar P, Preethi J, Vijayan R , et al. Anti-acne, anti-dandruff and anti-breast cancer efficacy of green synjournaled silver nanoparticles using Coriandrum sativum leaf extract[J]. Journal of Photochemistry & Photobiology B: Biology, 2016,163:69-76. |
[46] |
Onlom C, Khanthawong S, Waranuch N , et al. In vitro anti-Malassezia activity and potential use in anti-dandruff formulation of asparagus racemosus[J]. International Journal of Cosmetic Science, 2014,36(1) : 74-78.
doi: 10.1111/ics.12098 pmid: 24117781 |
[47] |
Park B M, Bak S S, Shin K O , et al. Promotion of hair growth by newly synthesized ceramide mimetic compound[J]. Biochemical & Biophysical Research Communications, 2017,491(1) : 173-177.
doi: 10.1016/j.bbrc.2017.07.069 pmid: 28711498 |
[48] |
Richena M, Rezende C A . Effect of photodamage on the outermost cuticle layer of human hair[J]. J Photochem Photobiol B, 2015,153:296-304.
doi: 10.1016/j.jphotobiol.2015.10.008 pmid: 26496793 |
[49] |
Ayako K, Tomoya T . Procyanidin B-3, isolated from barley and identified as a hair-growth stimulant, has the potential to counteract inhibitory regulation by TGF-beta1[J]. Experimental Dermatology, 2010,11(6) : 532-541.
doi: 10.1034/j.1600-0625.2002.110606.x pmid: 12473061 |
[50] |
Schmidt-Rose T, Braren S, Fölster H , et al. Efficacy of a piroctone olamine/climbazol shampoo in comparison with a zinc pyrithione shampoo in subjects with moderate to severe dandruff[J]. International Journal of Cosmetic Science, 2011,33(3) : 276-282.
doi: 10.1111/j.1468-2494.2010.00623.x pmid: 21272039 |
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