液相色谱-质谱法测定化妆品中10种邻苯二甲酸酯

doi:10.13218/j.cnki.csdc.2014.08.105

Abstract

Abstract: A method was established to determine residual content of phthalic acid esters (PAEs) in cosmetics.Samples were dissolved and then extracted under assistance of ultrasonic wave.Detection was performed using multiple reaction monitoring mode.The quantification was obtained utilizing the external standard method.Recoveries of residual content PAEs,with spike of ten times of the detection limit were 76.2%-95.2%,and the RSDs of the method were 4.4%-8.9%.The method can be applied to determine ten kinds of PAE in cosmetics simultaneously.

Key words: cosmetics, liquid chromatography-mass spectrometry (LC-MS), phthalic acid esters

CLC Number:

TQ658

BAI Ya-min, YANG Xiao-shan, MAO Qing, JIANG Sheng, QIN Jian. Determination of ten kinds of phthalic acid ester in cosmetics by LC-MS[J].China Surfactant Detergent & Cosmetics, 2014, 44(8): 472-475.

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Determination of ten kinds of phthalic acid ester in cosmetics by LC-MS

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