薰衣草纳米胶囊的制备、研究及应用

doi:10.3969/j.issn.1001-1803.2019.08.006

Abstract

Abstract:

The lavender fragrance nanocapsules were successfully prepared via the interfacial polymerization method using polyurea as the wall material to coat the lavender oil. Transmission electron microscope（TEM）images reveal that the nanocapsules possess regular spherical morphology with distinct core-shell structure, indicating that lavender oil is well encapsulated in the nanocapsules. And particle size distribution analysis shows that the average particle size of the lavender nanocapsules is approximately 131.7 nm with particle size distribution PDI of 0.16. Fourier transform infrared spectroscopy（FT-IR）and ultraviolet-visible analysis also show that the lavender oil can be well encapsulated inside the nanocapsules and the encapsulation efficiency of the nanocapules is as high as 96.5%. The thermal gravimetric analysis（TGA）and high temperature sustained-release curves indicate that the lavender oil encapsulated in the nanocapsules began to volatilize at 150 ℃ with good thermostability and sustained-release properties. Additionally, cotton fabrics treated with the fragrance nanocapsules display good washability after 150 min of soaping.

Key words: lavender oil, polyurea, nanocapsule, sustained release, fragrant fabric

CLC Number:

TQ655

YU Lin-lin,XIE Xing-hui,SHI Xiao-di,LI Xue-ting,LU Xi-hua. Preparation, characterization and application of lavender fragrance nanocapsules[J].China Surfactant Detergent & Cosmetics, 2019, 49(8): 519-525.

Figures/Tables 10

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References 15

[1]	Hu J, Deng W, Liu L , et al. Synjournal and application of polyacrylate nanocapsules loaded with lilial[J]. Journal of Applied Polymer Science, 2014,131(8) : 631-644.
[2]	Liu C, Liang B, Wang Y , et al. Core-shell nanocapsules containing essential oil for textile application[J]. Journal of Applied Polymer Science, 2017,135(4) : 45695.
[3]	Wang Yuqin, Sun Yajun, Shi Xianer . Chemical constituents and pharmacological activities of lavender essential oils[J]. Modern Medicine & Clinical Medicine, 2004,19(1) : 9-12.
[4]	Wang Aiqiong . Development of sustained-release microcapsules and its application on cotton fabrics[D]. Xi’an: Xi’an Polytechnic University, 2017.
[5]	Santos P P D, Flôres S H, Rios A D O , et al. Biodegradable polymers as wall materials to the synjournal of bioactive compound nanocapsules[J]. Trends in Food Science & Technology, 2016,53:23-33.
[6]	Yang Xiaolan, Yuan Ya, Tan Yurong , et al. Progress in the application of nano-microcapsule technology in functional foods[J]. Food Science, 2013,34(21) : 359-368.
[7]	Ge X T, Wan Z J, Song N , et al. Efficient methods for the extraction and microencapsulation of red pigments from a hybrid rose[J]. Journal of Food Engineering, 2009,94(1) : 122-128.
[8]	Oliveira C P, Venturini C G, Donida B , et al. An algorithm to determine the mechanism of drug distribution in lipid-core nanocapsule formulations[J]. Soft Matter, 2012,9(4) : 1141-1150.
[9]	Chu Hong, Yu Jia-de, Ni Zhong-bin , et al. Preparation of high-efficiency and slow-release aromatic plastics by microcapsule method[J]. China Plastics, 2013,27(2) : 60-64.
[10]	Martins I M, Barreiro M F, Coelho M , et al. Microencapsulation of essential oils with biodegradable polymeric carriers for cosmetic applications[J]. Chemical Engineering Journal, 2014,245(6) : 191-200.
[11]	Rodrigues S N, Martins I M, Fernandes I P , et al. Scentfashion (R) : Microencapsulated perfumes for textile application[J]. Chemical Engineering Journal, 2009,149(1-3) : 463-472.
[12]	Zhang H, Wang X . Synjournal and properties of microencapsulated n-octadecane with polyurea shells containing different soft segments for heat energy storage and thermal regulation[J]. Solar Energy Materials & Solar Cells, 2009,93(8) : 1366-1376.
[13]	Leclercq S, Harlander K R, Reineccius G A . Formation and characterization of microcapsules by complex coacervation with liquid or solid aroma cores[J]. Flavour & Fragrance Journal, 2010,24(1) : 17-24.
[14]	Zhao D, Jiao X, Zhang M , et al. Preparation of high encapsulation efficiency fragrance microcapsules and their application in textiles[J]. Rsc Advances, 2016,6(84) : 80924-80933.
[15]	Zhang Yao, Zhao Di , JiaoXin, et al. Preparation and characterization of polyurea as a capsule of peppermint oil microcapsules[J]. Acta Polymerica Sinica, 2016 ( 1) : 46-52.

Preparation, characterization and application of lavender fragrance nanocapsules

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