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日用化学工业 ›› 2020, Vol. 50 ›› Issue (1): 54-58.doi: 10.3969/j.issn.1001-1803.2020.01.010

• 分析与检测 • 上一篇    下一篇

氧化型染黑用途染发剂中32种染料监测结果分析

李彬,张伟清(),刘慧锦,侯俐南,乔亚森,王海燕()   

  1. 中国食品药品检定研究院,北京 100050
  • 收稿日期:2019-11-07 修回日期:2019-12-17 出版日期:2020-01-22 发布日期:2020-01-16
  • 通讯作者: 张伟清,王海燕
  • 作者简介:李 彬(1988-),女,工程师,工学硕士,电话:(010)67095054,E-mail: libin@nifdc.org.cn

Analysis on the determination results of 32 kinds of dyes used in oxidized blackening hair dyes

LI Bin,ZHANG Wei-qing(),LIU Hui-jin,HOU Li-nan,QIAO Ya-sen,WANG Hai-yan()   

  1. National Institutes for Food and Drug Control, Beijing 100050, China
  • Received:2019-11-07 Revised:2019-12-17 Online:2020-01-22 Published:2020-01-16
  • Contact: Wei-qing ZHANG,Hai-yan WANG

摘要:

采用《化妆品安全技术规范》(2015年版)中对苯二胺等32种组分的测定方法对市售25批氧化型染黑用途染发剂进行检测,并对组分检测结果、批件配方、标签标示三者进行比对,研究分析该类染发剂的生产和质量状况,发现风险点并提出合理的监管建议。结果表明,32种组分中涉及的8种禁用组分均未检出,24种准用染发剂组分中的苯基甲基吡唑啉酮有6批样品超限量添加,17批样品“检测结果与批件配方”不一致,16批样品“检测结果与标签标示”不一致,5批样品“批件配方与标签标示不一致;总体问题样品17批,问题发现率为68%。针对结果提出加强对含苯基甲基吡唑啉酮组分染发剂的监督抽检,开展包装、标签标示专项整顿的监管建议,并对超限量添加苯基甲基吡唑啉酮的原因进行分析。

关键词: 氧化型染黑用途染发剂, 批件配方, 标签标示, 苯基甲基吡唑啉酮, 监管建议

Abstract:

The 25 batches of commercially available oxidized blackening hair dyes were collected, and the contents of 32 selected chemical substances including p-Phenylenediamine in these products were assessed according to Safety and Technical Standards for Cosmetics (2015 edition). The content analysis results were compared with the approved formulas and labels of each product. The purpose of the survey was to gather information about the production and quality of this kind of hair dyes on domestic market, with the goal of uncovering the safety risks and providing supervision suggestions. The result shows that none of the eight prohibited components involved in the 32 components are detected in all investigated products. With regard to the 24 permitted hair dye components, phenyl methyl pyrazolone was found to exceed the permitted limit in 6 batches of the products. 17 batches of samples were inconsistent with the test results and the approved formulas, 16 batches of samples were inconsistent with the test results and the labels, and 5 batches of samples were inconsistent with the approved formulas and the labels. 17 batches of samples in total were problematic, with the problem discovery rate of 68%. According to the results, it is necessary to strengthen the inspection of hair dyes containing phenyl methyl pyrazolone, and carry out the special rectification in packages and labels. The reasons for the excessive addition of phenyl methyl pyrazolone was analyzed in the survey.

Key words: oxidized blackening hair dyes, approved formulas, labels, phenyl methyl pyrazolone, supervision suggestions

中图分类号: 

  • TQ658.3