抗菌纤维的抑菌活性及其在面膜产品中的应用研究

doi:10.3969/j.issn.2097-2806.2023.05.007

Abstract

Abstract:

To reduce irritant and toxicity risk effectively caused by traditional cosmetics preservatives, chitosan quaternary ammonium salt-based antibacterial fiber combined with several various bacteriostatic ingredients was constructed to replace the traditional preservatives used in facial mask products, which obviously improved its broad-spectrum antibacterial ability. The antibacterial properties of antibacterial fiber combined with a variety of antibacterial components were tested. The antibacterial effects comparison among quaternary ammonium chitosan antibacterial fiber combined with plant essential oil, traditional preservatives, and antiseptic substitutes on bacteria, yeast and mold was conducted. The several antiseptic recipes include antibacterial fiber and different antibacterial components were proposed. Antibacterial test results show that the antibacterial fiber combined with hydroxyacetophenone （0.1%-mass fraction, the same below）, or Eugenia caryophyllus Thunb. oil （0.05%）, or Leptospermum petersonii FM. Bailey oil, or Eucalyptus globulus Labill. oil, can meet the antibacterial requirements of mask products. However, the antibacterial fiber combined with methylparaben has antagonistic effect. Among them, the combination of antibacterial fiber with Eugenia caryophyllus Thunb. oil（0.05%） has the best antibacterial effect. The antibacterial fiber can significantly improve the antibacterial effect, and the improvement rate of Eugenia caryophyllus Thunb. oil is 43.06%.

Key words: antibacterial fiber, bacteriostatic performance, mask anticorrosion, essential oil, hydroxyacetophenone

CLC Number:

TQ658

Kong Qiuchan, Jiang Jiaxin, Xia Gaohui, Gong Shengzhao. Study on antibacterial activity of antibacterial fiber and its application in mask products[J].China Surfactant Detergent & Cosmetics, 2023, 53(5): 538-543.

Figures/Tables 8

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References 24

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抑菌圈宽度/mm	抑菌物质溶出性
≤1	非溶出性
>1~≤5	微溶出性
>5~≤10	中等溶出性
>10	高溶出性

细菌和酵母菌			真菌
菌种	抑菌率	抗菌效果	抑菌值A/培养后真菌数Tt	抗真菌效果
金黄色葡萄球菌	≥70%	有效	A<1	无效
大肠杆菌	≥70%	有效	1≤A<2	轻微抗菌
白色假丝酵母	≥60%	有效	2≤A<3	中等抗菌
铜绿假单胞菌	≥70%	有效	A≥3	全效抗菌
			Tt=0	杀真菌

类型	成分	编码	w/%
植物精油	丁香油	#1	0.03
	丁香油	#8	0.05
	茶树油	#2	0.03
	柠檬茶树油	#3	0.03
	柠檬茶树油	#9	0.05
	迷迭香叶油	#4	0.03
	蓝桉叶油	#5	0.03
	蓝桉叶油	#10	0.05
传统防腐剂	羟苯甲酯	#6	0.10
防腐替代剂	对羟基苯乙酮	#7	0.10
阳性对照	羟苯甲酯	#11	0.12
阳性对照	羟苯丙酯	#11	0.02

菌种	抑菌圈宽度/mm	抑菌物质溶出性
金黄色葡萄球菌	0	非溶出性
大肠杆菌	0	非溶出性
白色假丝酵母	0	非溶出性

细菌和酵母菌			真菌
菌种	抑菌率/%	抗菌效果	抑菌值A	抗真菌效果
金黄色葡萄球菌	92.14	有效	A=0.195	无效
大肠杆菌	93.75	有效
白色假丝酵母	63.64	有效
铜绿假单胞菌	90.00	有效

Study on antibacterial activity of antibacterial fiber and its application in mask products

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类型	编码	抑菌成分	抑菌率/%
植物精油	#1	丁香油	43.75
	#2	茶树油	26.25
	#3	柠檬茶树油	37.78
	#4	迭香叶油	26.25
	#5	蓝桉叶油	37.50
传统防腐剂	#6	羟苯甲酯	98.76
防腐替代剂	#7	对羟基苯乙酮	62.73
阳性对照	#11	羟苯甲酯+羟苯丙酯	>99.99

项目	菌种	初始值	7天	14天	21天	28天	结论
抗菌纤维+#8	混合细菌	5.3	<1	<1	<1	<1	通过
	白色假丝酵母	5.43	3.34	2.38	<1	<1	通过
	黑曲霉菌	5.04	4.38	4.04	3.66	3.28	通过
抗菌纤维+#9	混合细菌	5.3	4	<1	<1	<1	通过
	白色假丝酵母	5.43	3.38	3.08	2.12	1.42	通过
	黑曲霉菌	5.04	4.61	4.54	4.4O	3.66	通过
抗菌纤维+#10	混合细菌	5.3	3.42	<1	<1	<1	通过
	白色假丝酵母	5.43	4.29	4.2	4	3.86	通过
	黑曲霉菌	5.04	4.93	4.79	4.68	4.62	通过
抗菌纤维+#6	混合细菌	5.3	<1	<1	<1	<1	通过
	白色假丝酵母	5.43	5.72	5.20	5.08	4.95	不通过
	黑曲霉菌	5.04	5.4	4.96	5.14	5.02	不通过
抗菌纤维+#7	混合细菌	5.3	<1	<1	<1	<1	通过
	白色假丝酵母	5.43	5.11	5.01	3.62	<1	通过
	黑曲霉菌	5.04	5.00	4.56	4.12	3.75	通过
抗菌纤维+#11（阳性对照）	混合细菌	5.3	<1	<1	<1	<1	通过
	白色假丝酵母	5.43	<1	<1	<1	<1	通过
	黑曲霉菌	5.04	<1	<1	<1	<1	通过
抗菌纤维+基料（空白对照）	混合细菌	5.3	7.92	7.79	7.29	6.16	不通过
	白色假丝酵母	5.43	7.63	7.54	7.30	7.28	不通过
	黑曲霉菌	5.04	6.54	6.46	6.38	6.26	不通过

项目	抑菌率/%		提升率/%
项目	未使用抗菌纤维	使用抗菌纤维后	提升率/%
#6	98.76	17.27	-471.77
#7	62.73	67.27	6.75
#8	51.25	90.00	43.06
#9	48.89	68.18	28.30
#10	40.00	43.64	8.33

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