甘油和1，3-丁二醇在D相乳化法制备卸妆油中的应用研究

doi:10.3969/j.issn.1001-1803.2022.11.005

Abstract

Abstract:

The cleansing oil was prepared by D-phase emulsification method. PEG-20 glycerol triisostearate was selected as the emulsifier, glycerol or 1.3-butanediol was used as the co-emulsifier, and 10 kinds of oils in mineral oil, alkane and ester were selected. The effects of oils and polyols on the appearance, conductivity, microstructure and type of emulsion formed during D-phase emulsification were systematically analyzed. The research results show that: according to the ratio of fat∶emulsifier∶co-emulsifier （6∶3∶1）, it is found that mineral oil （7#, 10#）, ethylhexyl palmitate and two polyols can all form transparent cleansing oil system, but isohexadecane can only work with 1.3-butanediol to get the same system. By observing the appearance and electrical conductivity of the emulsion, it is found that the greater the interfacial tension between ester oils and glycerol, the higher the transparency of the formed system and the smaller the particle size. Compared with glycerin, 1.3-butanediol can improve the transparency of the microemulsion and the conductivity of the particles in the D-phase emulsification process, and it is easier to form a two-continuous phase structure, which can be used in a cleansing oil formulation system.

Key words: D-phase emulsification, PEG-20 glyceryl triisostearate, glycerin, 1.3-butanediol, cleansing oil

CLC Number:

TQ658

Dong Leilei, Huang Tianyi, Cai Yichao, Duan Guolan, Wu Xu, Zhou Qianhui, Zhang Dongmei. Research on the application of glycerin and 1.3-butanediol in the preparation of cleansing oil by D-phase emulsification method[J].China Surfactant Detergent & Cosmetics, 2022, 52(11): 1179-1187.

Figures/Tables 20

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References 13

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	组分	w/%	理论量/g
Part A	油脂	60	6
	PEG-20甘油三异硬脂酸酯	30	3
	多元醇	10	1
Part B	水	适量	适量

油脂类型	与甘油的界面张力/（mN/m）
棕榈酸乙基己酯	20.97±0.89
肉豆蔻酸异丙酯	17.00±0.08
甘油三（乙基己酸）酯	16.67±0.19
辛酸/癸酸甘油三酯	13.73±0.19

Research on the application of glycerin and 1.3-butanediol in the preparation of cleansing oil by D-phase emulsification method

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