China Surfactant Detergent & Cosmetics ›› 2024, Vol. 54 ›› Issue (10): 1260-1267.doi: 10.3969/j.issn.2097-2806.2024.10.014
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Han Qiao1,3,Mengxuan Wu1,3,Zihang Liu1,3,Shujun Cheng2,3,*()
Received:
2023-12-27
Revised:
2024-09-30
Online:
2024-10-22
Published:
2024-10-28
Contact:
E-mail: CLC Number:
Han Qiao, Mengxuan Wu, Zihang Liu, Shujun Cheng. Advances in laboratory methods for testing whitening efficacy of oral care products[J].China Surfactant Detergent & Cosmetics, 2024, 54(10): 1260-1267.
Tab. 2
Dyeing-cleaning cycle of tooth model"
参考文献 | 循环方式 |
---|---|
[ | 清洁4 h,人工唾液浸泡2 h,染色15 min,再浸入人工唾液17.75 h,一共24 h,持续22 d |
[ | 一过性染色后,将牛牙浸泡在酸性溶液中5 min,后直接进行刷磨720 轮,每轮200次往返,只进行一次 |
[ | 一过性染色后,将牛牙浸泡在酸性溶液中5 min,后置于人工唾液中15 min,后直接进行刷磨10 min |
[ | 一过性染色后,将牛牙浸泡在酸性溶液中10 min,后直接进行刷磨3 min,只进行一次 |
[ | 将标本暴露于10支香烟同时产生的烟雾中10 min,然后刷牙,一日一个周期 |
Tab. 3
Basic parameters of in vitro evaluation of whitening toothpaste"
参考文献 | 刷牙方式 | 刷磨次数(往返为一次) | 刷牙力 | 牙膏与水的比例 |
---|---|---|---|---|
[ | V8交叉刷牙机(V8 cross brushing machine) | 800次 | 150 g | 25 g∶40 mL(蒸馏水) |
[ | 自制刷牙机 | 100 000次(320 次/min) | ||
[ | 自制刷牙机,使用中等硬度的Exton纤维牙刷,在使用前已在水中浸泡16 h | 6~16 h(90 次/min) | 64~76 g | 1∶2 |
[ | BIOPDI自动刷牙机,软牙刷 | 5 d (90 次/d) | 150 g | 1∶3(人造唾液) |
[ | 交叉刷牙机(Cross brushing machine),直刷头 | 1 000次(200 次/min) | 150 g | |
[ | 手工刷牙,软刷毛,水平刷动 | 168 min | 1∶3 |
Tab. 4
Basic parameters of in vitro evaluation of whitening strips and gels"
研究 | 覆盖方式 | 处理时间 | 附加因素 |
---|---|---|---|
[ | 在牙齿颊面上均匀覆盖凝胶,结束后不洗去 | 每天2次,每次3 min,28 d | |
[ | 在牙齿颊面上均匀覆盖凝胶,结束后蒸馏水洗去 | 每疗程3次,每次15 min,共 3疗程,疗程间隔72 h | |
[ | 样品顶部放置增白条,测试间隔期间,将样本在流动的蒸馏水中冲洗1 min并浸入37 ℃蒸馏水中直到下一次处理 | 2 次/天,每次30 min,共21 d | |
[ | 使用乙酸乙烯酯乙酯板和真空机为每个样品制作一个厚度为1 mm的托盘。凝胶被施加到托盘中,并将托盘每天放置在每个样品上。完成每日漂白程序后,用去离子蒸馏水冲洗样品5 s | 每天6 h,21 d | |
[ | 涂敷试剂+光照刺激 | 每次15 min,4 次 | 15 min的前8 min用卤素灯照射/前30 s用激光照射 |
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