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China Surfactant Detergent & Cosmetics ›› 2024, Vol. 54 ›› Issue (10): 1227-1234.doi: 10.3969/j.issn.2097-2806.2024.10.010

• Development and application • Previous Articles     Next Articles

Preparation of PMTMS/TiO2 composite material and its performance characterization

Wanping Zhang,Xin Guan,Shilian Zheng,Dongmei Zhang,Zijia Zhang,Qianjie Zhang*()   

  1. Shanghai Institute of Technology, Shanghai 201418, China
  • Received:2024-03-12 Revised:2024-09-18 Online:2024-10-22 Published:2024-10-28
  • Contact: E-mail: zhangqj_sit@126.com.

Abstract:

To mitigate the aggregation behavior of TiO2 in organic system and also to enhance the synthesis efficiency of the composite carrier, methyltrimethoxysilane (MTMS) was used to coat TiO2. The surface morphology and properties of the coated PMTMS/TiO2 composites were characterized by the methods of FTIR, TGA, SEM, EDS, DLS, contact angle test, and lipophilicity test. The coating mechanism for PMTMS/TiO2 composites was summarized and elaborated. The results showed that the aggregation of PMTMS/TiO2 composites was greatly reduced when the synthesis condition was as follows: The mass ratio of MTMS to TiO2 was 3∶1, the mass fraction of catalyst was 1.9% and the reaction time was 5 h. The PMTMS/TiO2 composites thus prepared had good hydrophobicity. Therefore, by this way, the dispersion and compatibility of TiO2 particles in organic solvents were significantly improved.

Key words: titanium dioxide, polysiloxane, coating

CLC Number: 

  • TQ658