含陈皮提取物的氨基酸皂的制备及性能研究

doi:10.3969/j.issn.1001-1803.2020.06.009

Abstract

Abstract:

The “local authentic” medicinal material Xinhui tangerine peel was selected, and the flavonoids in tangerine peel were extracted by ultrasonic method as the active ingredients. The total flavonoid content and free radical scavenging ability in the tangerine peel extract were investigated. On this basis, a series of amino acid soaps containing tangerine peel extract were prepared by screening and compounding three kinds of amino acids, and their performance, antibacterial effect and efficacy were evaluated. The results show that the soaps containing tangerine peel extract are weakly acidic, with high transparency and hardness, good foaming and foam stabilizing properties, and have a certain ability to scavenge DPPH free radicals in a tangerine peel extract dose dependent manner. They also exhibited antibacterial activity against E.enteritidis and Staphylococcus aureus.

Key words: amino acid soap, tangerine peel extract, total flavonoids, foaming performance, antibacterial activity

CLC Number:

TQ423

LI Heng,JIANG Jia-huan,ZHONG Ying-xin,XU Zhao-hua,ZHENG Xiao-rui. Study on preparation and performance of amino acid soap containing tangerine peel extract[J].China Surfactant Detergent & Cosmetics, 2020, 50(6): 408-412.

Figures/Tables 7

Tab. 1

Tab. 2

Fig. 1

Tab. 3

Tab. 4

Fig. 2

Fig. 3

References 10

[1]	Zhang Wanping, Jiang Cheng. Preparation and technology of cosmetic products lecture series, second lecture: Non-sapon-based skin cleaning products[J]. Detergent & Cosmetics, 2018,41(11) : 54-60.
[2]	Mao Xuebin, Ge Zan, Shi Liwen, et al. Application progress of amino acid surfactants[J]. China Cleaning Industry, 2018 (10) : 44-47.
[3]	Li Heng, Xu Zhaohua, Jiang Jiahuan. A solid amino acid cleanser and its preparation: CN201910494964.9 [P]. 2019-06-10.
[4]	Wu Di. Extraction and anti-allergic activity of citri reticulatae pericarpium total flavonoids[D]. Changchun: Jilin University, 2016.
[5]	Sheng Zhaojun, Tan Yongquan, Ge Siyuan, et al. Quantitative determination of polyphenol contents comparison of antioxidant activities of extracts of Xinhui tangerine buds, green tangerine peel and tangerine peel[J]. Journal of Henan University of Technology (Natural Science Edition) , 2018,39(1) : 78-82.
[6]	Xu Xuyao. Studies on the determination of flavonoids and Vitamin C in citrus fruits[D]. Changsha: Hunan University, 2011.
[7]	Tan Xiaoyan, Yang Xiaoshan. Study on preparation of glutamic acid soap and lits performance[J]. China Cleaning Industry, 2019 (10) : 56-64.
[8]	Li Xiaoran, Mao Taoyan, Zheng Cheng, et al. Microwave-assisted extraction of tea seed saponin and its surface properties[J]. Fine Chemicals, 2018,35(8) : 1299-1305.
[9]	Tripathy D B, Mishra A, Clark J, et al. Synjournal, chemistry, physicochemical properties and industrial applications of amino acid surfactants: A review[J]. Comptes Rendus Chimie, 2018,21(2) : 112-130.
[10]	Wang Huifang, Shao Juan, Wang Man, et al. Preliminary study on extraction and antibacterial activity of total flavonoids in tangerine peel[J]. Science and Technology of Food Industry, 2018,39(8) : 130-135.

	原料	w/%
	原料	配方1	配方2	配方3	配方4	配方5
A相	椰油酰基谷氨酸	35	0	0	23	12
	月桂酰基谷氨酸	0	35	0	12	12
	肉豆蔻酰基谷氨酸	0	0	35	0	11
	丙三醇	10	10	10	10	10
	无水乙醇	10	10	10	10	10
	水	至100	至100	至100	至100	至100
B相	三乙醇胺	27	27	27	27	27

	原料	w/%
	原料	配方6	配方7	配方8	配方9
A相	椰油酰基谷氨酸	12	12	12	12
	月桂酰基谷氨酸	12	12	12	12
	肉豆蔻酰基谷氨酸	11	11	11	11
	丙三醇	10	10	10	10
	无水乙醇	7.5	5	2.5	0
	陈皮提取物	5	10	15	20
	水	至100	至100	至100	至100
B相	三乙醇胺	27	27	27	27

样品	PI/mm	透明度/%	pH
配方1	3.41	96.3	6.27
配方2	3.52	96.5	6.30
配方3	2.85	92.1	6.86
配方4	3.42	97.8	6.35
配方5	3.33	98.2	6.44
配方6	3.29	97.5	6.53
配方7	3.31	97.3	6.51
配方8	3.31	97.4	6.50
配方9	3.32	97.6	6.43
市售保湿水晶皂	3.34	97.7	6.38

样品	溶液刚流完时泡沫高度/mm	静置5 min后泡沫高度/mm
配方1	148	146
配方2	125	124
配方3	137.5	131
配方4	165	161.5
配方5	184	181.5
配方6	180	175
配方7	179	177
配方8	183	180.5
配方9	178	169
市售保湿水晶皂	70	10
K12溶液	203.5	201.5

[1]	Zhisheng Zhang, Chanliang Shen, Jianxun Li, Yanqiang Liu, Weiwei Han, Sanbao Dong. Preparation and performance of betaine/AOS/Gemini ternary surfactant foam for gas well deliquification [J]. China Surfactant Detergent & Cosmetics, 2024, 54(3): 239-249.
[2]	Zhang Peiliang, Yan Yongli, Lv Bo, Cao Yuxia, Wu Chunsheng, He Bingcheng. Experimental study on non-aqueous foams stabilized by CaCO₃ nanocrystals [J]. China Surfactant Detergent & Cosmetics, 2023, 53(6): 642-648.
[3]	Hao Qing, Wu Ermin, Bi Yongxian, Liu Jinjun, Kong Decheng, Cheng Zhiwei. Study on screening extraction process of total flavonoids from Nelumbinis Plumula by polyols and its properties [J]. China Surfactant Detergent & Cosmetics, 2023, 53(4): 398-407.
[4]	Yu Dongxiu,Jin Xiangxin,Liu Jiaxin,Li Junlang. Effects of nano-silver on the surface activity of triethanolammonium cocoyl glutamate [J]. China Surfactant Detergent & Cosmetics, 2022, 52(4): 363-369.
[5]	Zhang Xingqi,He Jingyu,Gong Shengzhao,Liu Linfeng. Study on the differences in the composition and the whitening and anti-allergy activities of different kinds of licorice [J]. China Surfactant Detergent & Cosmetics, 2021, 51(7): 648-654.
[6]	LIU Teng,ZHENG Yuan-lin,GE Ji-zhe,YANG Wei-dong,ZHANG Chao-zhong. Study on the effects of lipase on the detergency of the water-based ink-cleaner [J]. China Surfactant Detergent & Cosmetics, 2020, 50(2): 107-111.
[7]	JIA Ying,WANG Jia-min,WANG Shi-hui,LIU Kai-li,YANG Da-wei,WANG Yan. Study on the anti-inflammatory and antibacterial effects of compound radix arnebiae gel topical preparation [J]. China Surfactant Detergent & Cosmetics, 2020, 50(12): 848-853.
[8]	Yu-hao GUI,Xiao MENG,Qing-sheng CHEN,Sheng-zhao GONG. Study on antibacterial activity of plant essential oils and its application in cosmetics [J]. China Surfactant Detergent & Cosmetics, 2019, 49(3): 187-192.
[9]	LOU Shu-qin,XIA Wei,CHEN Lin-xiao,SONG Jin-xing,SUN Yi-shuo,ZHANG Wen-qing. Study on antibacterial property of clove complex extracted by different solvents [J]. China Surfactant Detergent & Cosmetics, 2019, 49(10): 649-655.
[10]	WANG Chen-chen, YI Yu-feng, SUN Chao, DING Fu-chen, MAO Rui-yun, HAN Jia. Properties of gas/liquid interfacial film formed by defoamer and its influence with respect to performance of the defoamer [J]. China Surfactant Detergent & Cosmetics, 2017, 47(1): 13-17.
[11]	REN Long-fang,SUN Yan-qing,LEI Sen. Preparation and foaming performance of sulfated tall oil surfactant [J]. China Surfactant Detergent & Cosmetics, 2016, 46(10): 561-564.
[12]	YANG Kai, ZHANG Gui-ju, XU Bao-cai. Process study on surfactant-assisted extraction of total flavonoids from Cistanche deserticola Y.C.Ma [J]. China Surfactant Detergent & Cosmetics, 2015, 45(6): 328-331.
[13]	TAN Fu-neng, SUI Wei-ping. Preparation and surface performance of O-hydroxypropyl-N-lauroyl chitosan [J]. China Surfactant Detergent & Cosmetics, 2015, 45(5): 252-256.
[14]	LIANG Qing, LI Wen-ru, SHI Qing-shan, ZHANG Wei-min. Analysis of components in Litsea cubeba oil and their effect for inhibition of putrilage bacteria in daily chemical products [J]. China Surfactant Detergent & Cosmetics, 2015, 45(5): 260-264.
[15]	LIU Wen-juan, CHANG Zhi-ying. Preservative efficacy and safety evaluation of antiseptic-free skin care cosmetics [J]. China Surfactant Detergent & Cosmetics, 2015, 45(4): 214-217.

Study on preparation and performance of amino acid soap containing tangerine peel extract

RichHTML

PDF (PC)

Like

Knowledge

Abstract

Cite this article

share this article

Figures/Tables 7

References 10

Related Articles 15

Metrics

Comments

Recommended 10