山茱萸多糖手工皂的工艺研究及安全性评价

doi:10.3969/j.issn.1001-1803.2019.04.009

Abstract

Abstract:

The handmade soap was prepared with the cold process using olive oil, coconut oil, palm oil and beeswax as soap base and polysaccharide of Corni Fructus as the functional component. The properties, antibacterial activity and safety of the soap were evaluated. The optimized proportions of coconut oil, palm oil, olive oil and beeswax were 25%, 25%, 45% and 5%, together with that of Corni Fructus polysaccharide being 1%. The indexes such as the total free base, free caustic alkali, water content and volatile oil were all consistent with the Chinese standards, and it was not irritant to the skin or eyes of rabbits. The results show that such handmade soap containing Corni Fructus polysaccharide is safe and nonirritating, which provides a scientific basis for utilization of the Corni Fructus.

Key words: handmade soap, polysaccharide of Corni Fructus, preparation process, safety evaluation

CLC Number:

TQ648

LIU Fang,ZHANG Qian,YANG Bin,HE Hua-kang,YANG Lei,GUO Chun-hua. Study on preparation process and safety evaluation of handmade soap containing Corni Fructus polysaccharide[J].China Surfactant Detergent & Cosmetics, 2019, 49(4): 248-252.

Figures/Tables 8

Tab.1

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References 17

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处方	w/%
处方	椰子油	棕榈油	橄榄油	蜜蜡
1	20	20	55	5
2	25	25	45	5
3	30	30	35	5

处方	总分/分
处方	泡沫细致度	泡沫持久度	泡沫浓密度	滋润度	清洁力
1	22	22	20	21	21
2	23	22	22	21	23
3	22	21	15	14	15

类别	w（测定值）/%				国家标准/%
类别	未加多糖	多糖1%	多糖2%	多糖4%	国家标准/%
总游离碱	0.167	0.201	0.193	0.184	≤0.3
游离苛性碱	0.069	0.070	0.072	0.070	≤0.1
水分和挥发物	1.666	2.020	2.269	3.701	≤30

组别	滴入1 h后			滴入24 h后			滴入48 h后			滴入72 h后
组别	结膜	巩膜	角膜	结膜	巩膜	角膜	结膜	巩膜	角膜	结膜	巩膜	角膜
对照组	0	0	0	0	0	0	0	0	0	0	0	0
未加多糖	0	0.5	0	0	0	0	0	0	0	0	0	0
1%多糖	0	0.5	0	0	0	0	0	0	0	0	0	0
2%多糖	0	0.7	0	0	0.5	0	0	0	0	0	0	0
4%多糖	0	0.5	0	0	0.2	0	0	0	0	0	0	0

Study on preparation process and safety evaluation of handmade soap containing Corni Fructus polysaccharide

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References 17

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w（多糖）/ %	总分/分
w（多糖）/ %	泡沫细致度	泡沫持久度	泡沫浓密度	滋润度	清洁力
0	23	22	22	21	23
1	27	25	24	23	21
2	22	23	20	20	22
4	20	20	14	14	15

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