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China Surfactant Detergent & Cosmetics ›› 2017, Vol. 47 ›› Issue (10): 593-597.doi: 10.13218/j.cnki.csdc.2017.10.012

• Analytical methods and testing • Previous Articles     Next Articles

Determination of eight heavy metal elements in cosmetics by super microwave digestion coupled with ICP-MS

HE Shuang, XUN Zhi-qing, HUANG Shao-man, LI Qiong, WU Chu-sen, YE Jia-rong   

  1. National Centre for Quality Supervision and Testing of Processed Food Guangzhou,Guangzhou Quality Supervision and Testing Institute,Guangzhou,Guangdong 511447,China
  • Received:2017-06-30 Published:2019-03-21

Abstract: A method for determination of eight heavy metal elements including chromium,nickel,cobalt,vanadium,molybdenum,antimony,thallium and lead in various cosmetics was established by using super microwave digestion and inductively coupled plasma-mass spectrometry (ICP-MS).The samples were digested with nitric acid-water system under assistance of super microwave irradiation,detected by ICP-MS and quantified by external standard method.Under the optimized conditions,good linear relationships of eight heavy metals are showed within the mass concentration range of 0-100 μg/L with the correlation coefficient larger than 0.999.The detection limits of the method are not higher than 0.012 mg/kg.This method has been successfully applied to the detection and analysis of eight heavy metal elements in various kinds of cosmetics.The recoveries of the spiked samples are between 88.5%-108.5% with the relative standard deviation not more than 3.89%.This method is simple,accurate and precision,which provides an effective method for the rapid determination of eigth heavy metals in various cosmetics.

Key words: cosmetics, super microwave, ICP-MS, heavy metal

CLC Number: 

  • TQ658